Ethyl bromoacetate → HCID 18316767, 화합물
반응식
Br.[Br:2][CH2:3][CH2:4][C:5]1[CH:11]=[CH:10][C:8]([NH2:9])=[CH:7][CH:6]=1.C(=O)([O-])[O-].[K+].[K+].Br[CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21]>CN(C)C=O>[Br:2][CH2:3][CH2:4][C:5]1[CH:11]=[CH:10][C:8]([NH:9][CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])=[CH:7][CH:6]=1참가 물질
5
실험 절차
To a solution of 4-(2-bromoethyl)aniline hydrobromide (9.15 g) in N,N-dimethylformamide (65 ml) were added potassium carbonate (4.95 g) and ethyl bromoacetate (3.97 ml), and the mixture was stirred for 36 hours at room temperature. The reaction mixture was poured into ice-water, and collection of the resulting precipitates by filtration gave ethyl N-[4-(2-bromoethyl)phenyl]aminoacetate (8.39 g)
후처리
- customprecipitates by filtration
출처 및 근거
- ORD 기록
- ord-087c87c3a38a4d92a16aaded4ddc1558
- 출처 데이터셋
- uspto-grants-2002_03
- 특허 번호
- US06353025B1
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