Thionyl Chloride → HCID 18316160, 화합물
반응식
[CH:1]1([NH:6][CH2:7][CH2:8]O)[CH2:5][CH2:4][CH2:3][CH2:2]1.O=S(Cl)[Cl:12]>>[CH:1]1([NH:6][CH2:7][CH2:8][Cl:12])[CH2:5][CH2:4][CH2:3][CH2:2]1참가 물질
3
실험 절차
2-Hydroxyethylamine and cyclopentanone were reacted according to Method B4b, Step 1 to afford 4-aza-1-oxaspiro[4.4]nonane. The oxazolidine was reduced according to method B4b, Step 2 to afford N-cyclopentyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to afford N-cyclopentyl-N-(2-chloroethyl)amine. The amine was reacted with 2,3-dichlorophenyl isothiocyanate according to Method C1d to afford 2-(2,3-dichlorophenylimino)-3-cyclopentyl-1,3-thiazolidine.
출처 및 근거
- ORD 기록
- ord-a43bd6f7f8eb400792432c53017a843f
- 출처 데이터셋
- uspto-grants-2002_03
- 특허 번호
- US06353006B1
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