2,3-Dichlorophenyl Isothiocyanate → 2-(2,3-Dichlorophenylimino)-3-cyclooctyl-1,3-thiazolidine

HRID 276343

반응식

HRID 276343 반응식
[Cl-].[CH:2]1([NH2+:10][CH2:11][CH2:12]Cl)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[Cl:14][C:15]1[C:20]([Cl:21])=[CH:19][CH:18]=[CH:17][C:16]=1[N:22]=[C:23]=[S:24]>>[Cl:14][C:15]1[C:20]([Cl:21])=[CH:19][CH:18]=[CH:17][C:16]=1[N:22]=[C:23]1[N:10]([CH:2]2[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]2)[CH2:11][CH2:12][S:24]1

참가 물질

3

반응물 2

HCID 27962812,3-Dichlorophenyl IsothiocyanateHCID 18316362N-cyclooctyl-N-(2-chloroethyl)ammonium chloride

생성물 1

HCID 183161712-(2,3-Dichlorophenylimino)-3-cyclooctyl-1,3-thiazolidine

실험 절차

2-Hydroxyethylamine was reacted with cyclooctyl bromide according to Method B2a to give N-cyclooctyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclooctyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 2,3-dichlorophenyl isothiocyanate to give 2-(2,3-dichlorophenylimino)-3-cyclooctyl-1,3-thiazolidine.

출처 및 근거

ORD 기록
ord-afe4030e78884949996ae2efa0f45ffc
출처 데이터셋
uspto-grants-2002_03
특허 번호
US06353006B1

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