1,2-Dichloro-4-isothiocyanatobenzene → 2-(3,4-Dichlorophenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine

HRID 276372

반응식

HRID 276372 반응식
[Cl-].[CH:2]1([CH2:7][NH2+:8][CH2:9][CH2:10]Cl)[CH2:6][CH2:5][CH2:4][CH2:3]1.[Cl:12][C:13]1[CH:14]=[C:15]([N:20]=[C:21]=[S:22])[CH:16]=[CH:17][C:18]=1[Cl:19]>>[Cl:12][C:13]1[CH:14]=[C:15]([N:20]=[C:21]2[N:8]([CH2:7][CH:2]3[CH2:3][CH2:4][CH2:5][CH2:6]3)[CH2:9][CH2:10][S:22]2)[CH:16]=[CH:17][C:18]=1[Cl:19]

참가 물질

3

반응물 2

HCID 230651,2-Dichloro-4-isothiocyanatobenzeneHCID 18316280N-cyclopentylmethyl-N-(2-chloroethyl)ammonium chloride

생성물 1

HCID 183162972-(3,4-Dichlorophenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine

실험 절차

2-Hydroxyethylamine was reacted with cyclopentylmethyl bromide according to Method B2a to give N-cyclopentylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclopentylmethyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 3,4-dichlorophenyl isothiocyanate to give 2-(3,4-dichlorophenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine.

출처 및 근거

ORD 기록
ord-7d4e12a7032a427aa23651c4440c29e5
출처 데이터셋
uspto-grants-2002_03
특허 번호
US06353006B1

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