Thionyl Chloride → HCID 18316241, 화합물

HRID 276394노트

반응식

C1(C(N)C)CCCCC1.O[CH2:11][CH2:12][NH:13][CH:14]([CH:16]1[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1)[CH3:15].O=S(Cl)[Cl:24]>>[Cl-:24].[Cl:24][CH2:11][CH2:12][NH2+:13][CH:14]([CH:16]1[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1)[CH3:15]

참가 물질

반응물 3

HCID 24386Thionyl Chloride

HCID 1107331-Cyclohexylethylamine

HCID 18316436HCID 18316436, 화합물

생성물 1

HCID 18316241HCID 18316241, 화합물

실험 절차

1-Cyclohexyl-1-ethylamine was converted to N-(2-hydroxyethyl)-N-(1-cyclohexyl-1-ethyl)amine according to Method B5a. The alcohol was reacted with SOCl2 according to Method B7a to give N-(2-chloroethyl)-N-(1-cyclohexyl -1-ethyl)ammonium chloride. The chloroethylamine was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give 2-(2-methyl-4-nitrophenylimino)-3-(1-cyclohexyl-1-ethyl)-1,3-thiazolidine.

출처 및 근거

ORD 기록: ord-9c8d6022a0b54b27b6657b1e4b9502ca
출처 데이터셋: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06353006B1

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