Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanolamine → N-(2-hydroxyethyl)-N-(cyclododecylmethyl)amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanolamine | HCID 700 | — |
| 반응물 | Cyclododecanemethanol | HCID 74686 | — |
| 반응물 | Cyclododecylmethylbromide | HCID 18316415 | — |
| 생성물 | N-(2-hydroxyethyl)-N-(cyclododecylmethyl)amine | HCID 18316365 | — |
반응 단계
Methyl cyclododecanecarboxylate was reduced according to Method B2b, Step 1 to give cyclododecylmethanol. The alcohol was converted to cyclododecylmethylbromide according to Method B2b, Step 2. The halide was reacted with 2-hydroxyethylamine according to Method B2b, Step 3 to give N-(2-hydroxyethyl)-N-(cyclododecylmethyl)amine. The alcohol was reacted with SOCl2 according to Method B7a to give N-(2-chloroethyl)-N-(cyclododecylmethyl)ammonium chloride. The chloroethylamine was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give 2-(2-methyl-4-nitrophenylimino)-3-(cyclododecylmethyl)-1,3 -thiazolidine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06353006B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-981e06a11c21447db0d13bd451d53b47 |
| 출처 메모 | uspto-grants-2002_03 |