Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanolamine → 9-(2-Methyl-4-nitrophenylimino)-1-aza-8-thiabicyclo[4.3.0]nonane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanolamine | HCID 700 | — |
| 반응물 | 2-Methyl-4-nitrophenyl isothiocyanate | HCID 145621 | — |
| 반응물 | Methyl pipecolinate | HCID 3463753 | — |
| 반응물 | HCID 178478436 | HCID 178478436 | — |
| 생성물 | 9-(2-Methyl-4-nitrophenylimino)-1-aza-8-thiabicyclo[4.3.0]nonane | HCID 18316305 | — |
반응 단계
2-Piperidenemethanol was made from methyl pipecolinate as described in Method B1b. The 2-hydroxyethylamine was converted to 2-chloromethylpiperidinium chloride according to Method B7a. 2-Methyl4-nitrophenyl isothiocyanate was reacted with 2-chloromethylpiperidinium chloride according according to Method C1a to give 9-(2-methyl-4-nitrophenylimino)-1-aza-8-thiabicyclo[4.3.0]nonane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06353006B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-c951ff5debe4466ebad410dd29a6a027 |
| 출처 메모 | uspto-grants-2002_03 |