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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 276651생성일: 2026년 10월 27일

Cyclohexyl bromide → 1-Cyclohexyl-2-(2-methyl-4-nitrophenylimino)-3-thia-1-azaspiro[4.4]nonane

https://huagongshe.com/reaction/276651

반응식

참여 물질

역할이름HCID투입량
반응물Cyclohexyl bromideHCID 7960—
반응물2-(2-Methyl-4-nitrophenylimino)-3-thia-1-azaspiro[4.4]nonaneHCID 178428736—
생성물1-Cyclohexyl-2-(2-methyl-4-nitrophenylimino)-3-thia-1-azaspiro[4.4]nonaneHCID 9907571—

반응 단계

1-Hydroxymethylcyclopentanamine was prepared according to Method B1c. The 2-hydroxyethylamine was sequentially reacted with SOCl2 and 2-methyl-4-nitrophenyl isothiocyanate according to Method C2a to give 2-(2-methyl-4-nitrophenylimino)-3-thia-1-azaspiro[4.4]nonane. The thiazolidine was reacted with cyclohexyl bromide according to Method D2e to give 2-(2-methyl-4-nitrophenylimino)-1-cyclohexyl-3-thia-1-azaspiro[4.4]nonane.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06353006B1
출처 데이터셋uspto-grants-2002_03
ORD IDord-2d0bbd55614c49b8a02aecb33bdef523
출처 메모uspto-grants-2002_03