Isobutylamine → 2-(2-Methyl-4-nitrophenylimino)-3-isobutyl-5-phenyl-1,3-thiazolidin-4-one

HRID 276673

반응식

[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]=[S:13].[CH2:14]([NH2:18])[CH:15]([CH3:17])[CH3:16].Cl[CH:20]([C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[C:21](O)=[O:22]>>[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]1[N:18]([CH2:14][CH:15]([CH3:17])[CH3:16])[C:21](=[O:22])[CH:20]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[S:13]1

참가 물질

반응물 3

HCID 6558Isobutylamine

HCID 98950Chloro(phenyl)acetic acid

HCID 1456212-Methyl-4-nitrophenyl isothiocyanate

생성물 1

HCID 183162222-(2-Methyl-4-nitrophenylimino)-3-isobutyl-5-phenyl-1,3-thiazolidin-4-one

실험 절차

2-Methyl-4-nitrophenyl isothiocyanate was reacted with isobutylamine followed by α-chloro-α-phenylacetic acid according to Method C8a to afford 2-(2-methyl-4-nitrophenylimino)-3-isobutyl-5-phenyl-1,3-thiazolidin4-one.

출처 및 근거

ORD 기록: ord-dcd943bc227f43dc96f18aaddca3fc65
출처 데이터셋: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06353006B1

연결된 노트

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