Triethylamine → N-(3-benzoylphenyl)-4-chlorobenzamide

HRID 27723노트

반응식

HRID 27723 반응식
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][CH:3]=1.[NH2:11][C:12]1[CH:13]=[C:14]([CH:23]=[CH:24][CH:25]=1)[C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16].C(N(CC)CC)C>CC(N(C)C)=O>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH:11][C:12]2[CH:13]=[C:14]([CH:23]=[CH:24][CH:25]=2)[C:15]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[O:16])=[O:7])=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 85014-Chlorobenzoyl chlorideHCID 17817Methanone, (3-aminophenyl)phenyl-

생성물 1

HCID 721817N-(3-benzoylphenyl)-4-chlorobenzamide

시약·촉매·용매 1

HCID 31374Dimethylacetamide용매

실험 절차

With agitation, 4.9 g 4-chlorobenzoyl chloride are added bit by bit to a solution, cooled to 5° C., of 5 g 3-amino-benzophenone in 60 ml dimethylacetamide, in the presence of 4.9 g triethylamine.

출처 및 근거

ORD 기록
ord-a9355115fe224833bb176592d5ae49f2
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04223039

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