Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → HCID 22625376, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | ((p-(Benzyloxy)phenoxy)methyl)oxirane | HCID 119882 | — |
| 반응물 | 1-(2,5-Dimethoxyphenyl)piperazine dihydrochloride | HCID 13599003 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | HCID 22625376 | HCID 22625376 | 33.9% |
반응 단계
2.56 g of 1-(4-benzyloxyphenoxy)-2,3-epoxypropane was dissolved in 100 ml of dioxane, and to this were added 2.95 g of 1-(2,5-dimethoxyphenyl)piperazine dihydrochloride and 3.5 ml of triethylamine and reaction and workup were carried out as in Example 1-A. The residue obtained was purified by column chromatography (silica gel, elution with ethyl acetate:hexane=1:1) to give 1.62 g of brown oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06358515B2 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-74ab6cf6ea5342a989d4f284f57cbbbb |
| 출처 메모 | uspto-grants-2002_03 |