Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → HCID 22625351, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | ((p-(Benzyloxy)phenoxy)methyl)oxirane | HCID 119882 | — |
| 반응물 | HCID 22625378 | HCID 22625378 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | HCID 22625351 | HCID 22625351 | 67.3% |
반응 단계
Using 1.56 g of 1-(4-benzyloxyphenoxy)-2,3-epoxypropane, 1.80 g of 1-(2,4-dimethoxyphenyl)piperazine dihydrochloride, 1.9 ml of triethylamine and 50 ml of dioxane, reaction and workup were carried out as in Example 1-A. Purification by column chromatography (silica gel, elution with ethyl acetate:hexane =1:0.5) gave 1.96 g of pale red crystals, m.p. 110-112° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06358515B2 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-0f1cbbe117464338a1abcdc98b305f2c |
| 출처 메모 | uspto-grants-2002_03 |