Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tributyl(prop-1-yn-1-yl)stannane → Methyl 3-benzyloxycarbonylamino-4-(1-propynyl)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tributyl(prop-1-yn-1-yl)stannane | HCID 2733165 | — |
| 반응물 | 2-Benzyloxycarbonylamino-4-methoxycarbonylphenyl trifluoromethanesulfonate | HCID 22627443 | — |
| 생성물 | Methyl 3-benzyloxycarbonylamino-4-(1-propynyl)benzoate | HCID 22627370 | 85.5% |
반응 단계
Methyl 3-benzyloxycarbonylamino-4-(1-propynyl)benzoate (1.34 g) was prepared from 2-benzyloxycarbonylamino-4-methoxycarbonylphenyl trifluoromethanesulfonate (2.1 g) and tributyl (1-propynyl)stannane (2.49 g) in a similar manner to that of Preparation 1 (2).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06358992B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-4adf7ce23f2d49fd9d9e73f8fc9f8dfc |
| 출처 메모 | uspto-grants-2002_03 |