참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Diisopropyl Ether | HCID 7914 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Anthranilic acid, 3-hydroxy-, methyl ester | HCID 205248 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | Methyl 2-acetamido-3-acetoxybenzoate | HCID 22627220 | — |
반응 단계
To a solution of methyl 2-amino-3-hydroxybenzoate (882 mg) in pyridine (2 ml) was added acetic anhydride (1.2 ml) and the mixture was stirred at 20° C. for 8 hours. The reaction mixture was diluted with diisopropyl ether, and the resulting solid was collected and washed with diisopropyl ether. The solid was triturated with diisopropyl ether to give methyl 2-acetamido-3-acetoxybenzoate (1.25 g) as solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06358992B1 |
|---|
| 출처 데이터셋 | uspto-grants-2002_03 |
|---|
| ORD ID | ord-220fb2030ea249dfb5f93ee57b7c112a |
|---|
| 출처 메모 | uspto-grants-2002_03 |
|---|
