Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Prop-2-enimidic acid--2-(dimethylamino)ethyl 2-methylprop-2-enoate (1/1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Acrylamide | HCID 6579 | — |
| 반응물 | (Dimethylamino)ethyl methacrylate | HCID 17869 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Prop-2-enimidic acid--2-(dimethylamino)ethyl 2-methylprop-2-enoate (1/1) | HCID 160008 | — |
반응 단계
To a solution of 50.0 grams of acetic acid in 350 grams of water is added 131 grams of DMAEMA followed by 119 grams of acrylamide. The pH of the solution is 7.0 without any adjustment. The rest of the procedure is the same as followed in Example A. After 5 hours G.L.C. analysis showed there was no DMAEMA monomer remaining, while 33% of the acrylamide was recovered. This indicates that ≈66% of the DMAEMA had been quaternized.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04224150 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-414dbc5005a144c69fd585ed4937b365 |
| 출처 메모 | uspto-grants-1980_09 |