Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
m-(Dimethylamino)benzyl alcohol → 3-(Dimethylamino)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | m-(Dimethylamino)benzyl alcohol | HCID 90133 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3-(Dimethylamino)benzaldehyde | HCID 34288 | 72% |
반응 단계
The same installation as in Example 1 is used. Using a similar method to Example 1, a mixture of 320 parts of m-dimethylaminobenzyl alcohol and 50 parts of water with 300 parts of air is passed per hour over the catalyst at 530° C. and 1.2 bar. The residence time is 0.035 second and the throughput 0.45 tonne/m2.h. 228 parts of m-dimethylaminobenzaldehyde (in the form of an 88 percent strength by weight organic phase) are obtained per hour, corresponding to a yield of 72% of theory. The conversion is 94 percent and the space-time yield is 11 grams of m-dimethylaminobenzaldehyde per cm3 of catalyst volume per hour.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04224254 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-47d5a9d6c7484b189cf7efd4b9713e96 |
| 출처 메모 | uspto-grants-1980_09 |