Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,4-Benzenedimethanol → Terephthalaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,4-Benzenedimethanol | HCID 11506 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | Terephthalaldehyde | HCID 12173 | 63% |
반응 단계
Using a similar method to Example 1, a mixture of 200 parts of 4-(hydroxymethyl)-benzyl alcohol and 400 parts of dioxane with 290 parts of air is passed per hour over the catalyst at 600° C. and 1.1 bar. The residence time is 0.05 second and the throughput is 0.3 tonne/m2.h. 124 parts of terephthaldialdehyde (in the form of a 22 percent strength by weight solution) are obtained per hour, corresponding to a yield of 63% of theory. The conversion is 92 percent and the space-time yield is 6 grams of terephthaldialdehyde per cm3 of catalyst volume per hour.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04224254 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-e2d4d36db43f4530ae0c426fa7c10af8 |
| 출처 메모 | uspto-grants-1980_09 |