Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pivalic acid → n-Neopentanoyl-2-butyloctylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pivalic acid | HCID 6417 | — |
| 반응물 | 2-Butyl-n-octan-1-amine | HCID 18673284 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | n-Neopentanoyl-2-butyloctylamine | HCID 18673286 | 76% |
반응 단계
10.4 g of pivalic acid and 17.2 g of 2-butyloctylamine were mixed together in the tube of a microwave machine (Maxidigest™ MX 350 from the company Prolabo; frequency 2450±50 MHz, modulable power 300 W). After irradiation for about 1 hour at 160° C.±10° C., the reaction mixture was dissolved in heptane and then purified on silica. 19 g of the desired amide were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06359175B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-8b27d062e00d4dcfacb35b68adc53cff |
| 출처 메모 | uspto-grants-2002_03 |