Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5,5-Trimethylhexanoic acid → n-(3,5,5-Trimethylhexanoyl)-2-octyldodecylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5,5-Trimethylhexanoic acid | HCID 90960 | — |
| 반응물 | 2-n-Octyl-1-dodecylamine | HCID 18761999 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | n-(3,5,5-Trimethylhexanoyl)-2-octyldodecylamine | HCID 18673283 | — |
반응 단계
3.6 g of 3,5,5-trimethylhexanoic acid and 6.8 g. of 2-octyldodecylamine were mixed together in the tube of a microwave machine (Maxidigest™ MX 350 from the company Prolabo; frequency 2450±50 MHz, modulable power 300 W). After irradiation for about 50 minutes at 170° C.±10° C., the reaction mixture was dissolved in heptane and then purified on silica. 7 g of the desired amide were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06359175B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-0f09de70df754ed39b82a2c0ae0c94c3 |
| 출처 메모 | uspto-grants-2002_03 |