Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5,5-Trimethylhexanoic acid → n-(3,5,5-Trimethylhexanoyl)-2-butyloctylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5,5-Trimethylhexanoic acid | HCID 90960 | — |
| 반응물 | 1400w Dihydrochloride | HCID 2733515 | — |
| 반응물 | 2-Butyl-n-octan-1-amine | HCID 18673284 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | n-(3,5,5-Trimethylhexanoyl)-2-butyloctylamine | HCID 18673287 | 77% |
반응 단계
29.2 g of 3,5,5-trimethylhexanoic acid and 34.2 g of 2-butyloctylamine were mixed together in an open Pyrex container and placed in a microwave oven (Menumaster™3100 i; frequency 2450, power at a setting of 30%: 1400 W). After 6 irradiations of about 5 minutes (for each irradiation), the reaction mixture was dissolved in heptane and then purified on silica. 46 g (77%) of the desired amide were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06359175B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-5fb2aa7435834a2a9de928fec37e62b3 |
| 출처 메모 | uspto-grants-2002_03 |