Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl fluoride, 4-(trifluoromethoxy)- → 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl fluoride, 4-(trifluoromethoxy)- | HCID 67612 | — |
| 반응물 | 1,8-Diaminonaphthalene | HCID 68067 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE | HCID 12945439 | — |
반응 단계
1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04224326 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-ef9f817d260c40a48ed57129ebeb83cc |
| 출처 메모 | uspto-grants-1980_09 |