Toluene ethanol → 2,3,4,5,11,15b-hexahydro-2,8-dimethyl-1H-dibenz[3,4:6,7]azepino[1,2-a](1,4)diazepine
반응식
[CH3:1][N:2]1[CH2:22][CH2:21][CH2:20][N:5]2[C:6]3[CH:18]=[C:17]([CH3:19])[CH:16]=[CH:15][C:7]=3O[C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[CH:4]2[CH2:3]1.[C:23]1(C)C=CC=CC=1.C(O)C>>[CH3:1][N:2]1[CH2:22][CH2:21][CH2:20][N:5]2[C:6]3[CH:18]=[C:17]([CH3:19])[CH:16]=[CH:15][C:7]=3[CH2:23][C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[CH:4]2[CH2:3]1참가 물질
3
실험 절차
1,2,3,4,5,15b-hexahydro-2,8-dimethyl-1,4-diazepino[1,2-d]dibenz[b,f](1,4)oxazepine, (oil) Rf in toluene:ethanol (8:2)=0.42 on SiO2 ;
출처 및 근거
- ORD 기록
- ord-2255452c96d541f5a4c2c2a1e4e2e403
- 출처 데이터셋
- uspto-grants-1980_09
- 특허 번호
- US04224321
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