Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Aminonaphthalene-1,8-dicarboxylic anhydride → 6-Amino-2-hydroxy-benzo[de]isoquinoline-1,3-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Aminonaphthalene-1,8-dicarboxylic anhydride | HCID 80990 | — |
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 6-Amino-2-hydroxy-benzo[de]isoquinoline-1,3-dione | HCID 15896245 | 97.4% |
반응 단계
4-Amino-1,8-naphthalic anhydride (0.2 g, 0.9 mmol) and hydroxylamine hydrochloride (0.1 g, 1.4 mmol) were reacted in pyridine (20 mL) following the procedure of Example 1 to give 0.2 g of the title compound, mp >360° C.;
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362181B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-5c6e1141e8ca4934b1d04089a796f586 |
| 출처 메모 | uspto-grants-2002_03 |