Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(Trifluoromethyl)aniline → 3-oxo-N-[3-(trifluoromethyl)phenyl]butanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(Trifluoromethyl)aniline | HCID 7375 | — |
| 반응물 | Diketene | HCID 12661 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 3-oxo-N-[3-(trifluoromethyl)phenyl]butanamide | HCID 744366 | — |
반응 단계
m-Trifluoromethyl aniline (32.22 g) in benzene was dissolved in benzene and diketene added slowly with mixing. The reaction mixture was allowed to stand at 25° C. The resulting solid product was recrystallized from ethanol to yield 3'-trifluoromethyl acetoacetanilide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04224334 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-e2e79f9094af4c188695b3e1de86223b |
| 출처 메모 | uspto-grants-1980_09 |