Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Indanone → 3-Bromo-1-indanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Indanone | HCID 6735 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 3-Bromo-1-indanone | HCID 11745912 | — |
반응 단계
1-Indanone (1 g) and NBS (1.4 g) was mixed with dry CCl4 (20 ml). A catalytic amount of AlBN was added and the mixture was refluxed for 30 minutes and excited with light using 250 W lamp. The mixture was cooled in an ice bath and filtered. The filtrate was concentrated in an evaporator and used without further purification for the next step. Yield was 1.5 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362211B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-c54a0fd89f4a4e89ae60c4b36eb93b67 |
| 출처 메모 | uspto-grants-2002_03 |