Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylene Oxide → Diglycidyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylene Oxide | HCID 6354 | — |
| 반응물 | Epichlorohydrin | HCID 7835 | — |
| 반응물 | 1-Tetradecanol | HCID 8209 | — |
| 반응물 | Tin tetrachloride | HCID 24287 | — |
| 생성물 | Diglycidyl ether | HCID 16704 | — |
반응 단계
One mole of tetradecanol ethoxylated with 2 moles of ethylene oxide per mole of tetradecanol and one mole of epichlorohydrin were reacted in the presence of tin tetrachloride at a temperature of 60 to 70° C. and a glycidyl ether was obtained. A solution of 30% sodium hydroxide in water was added at 80° C. After 30 minutes under vigorous stirring at 80° C., the resulting glycidyl ether was separated from the water phase. It had the structure
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362238B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-551345e6ed0d48d895c3e31df8f1b3d3 |
| 출처 메모 | uspto-grants-2002_03 |