Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
8-Hydroxyquinoline → Zinc oxyquinolate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 8-Hydroxyquinoline | HCID 1923 | — |
| 반응물 | Zinc acetate (USP) | HCID 2724192 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Zinc oxyquinolate | HCID 84127 | 89.4% |
반응 단계
Zinc acetate dihydrate (1.0 g) was dissolved in 75 ml. of hot methanol and 1.4 g of 8-hydroxyquinoline was added to the homogeneous solution. A yellow precipitate formed after a few minutes and the solution was stirred at reflux for 3 hours. The solution was allowed to cool and the precipitate was isolated by filtration and washed with methanol and petroleum ether. After air drying, 1.44 g of bis(8-hydroxyquinolinato)zinc was obtained as a bright yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362339B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-abc429fc50e549d38327d32c4b5108cd |
| 출처 메모 | uspto-grants-2002_03 |