Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 22624891, 화합물 → 2-(Pyridin-3-yloxy)ethan-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 22624891 | HCID 22624891 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-(Pyridin-3-yloxy)ethan-1-ol | HCID 21908997 | 86% |
반응 단계
A solution of 3-(2-(tetrahydropyran-2-yloxy)ethoxy)pyridine (1.54 g, 7 mmol) in acetic acid (8 ml), THF (4 ml) and water (2 ml) was heated at 50° C. for 4 hours. The volatiles were removed by evaporation and the residue azeotroped with toluene to give 3-(2-hydroxyethoxy)pyridine (820 mg, 86%) as an off-white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362336B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-27d37db75bc147aaac8aa4d41bb8802f |
| 출처 메모 | uspto-grants-2002_03 |