Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1H-Imidazole-4,5-dicarboxylic acid, 4,5-dimethyl ester → 1H-Imidazole-4,5-dimethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1H-Imidazole-4,5-dicarboxylic acid, 4,5-dimethyl ester | HCID 76810 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1H-Imidazole-4,5-dimethanol | HCID 573629 | — |
반응 단계
Reflux dimethyl 4,5 imidazole dicarboxylate (1.8 g) in THF (tetrahydrofuran) with 2.5 equivalents of LAH lithium aluminum hydride). Neutralize with NH4Cl solution and filter. Concentrate the filtrate under vacumm and extract the product with ethanol. Remove the solvent, filtrate through alumina using a THF solvent to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04587241 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-12483586f11b49f08bb683b241c74f50 |
| 출처 메모 | uspto-grants-1986_05 |