Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl carbazate → N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl carbazate | HCID 80519 | — |
| 반응물 | 2-Benzylcyclohexan-1-one | HCID 98945 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine | HCID 57106415 | 96.9% |
반응 단계
18.83 g (0.1 mole) of 2-benzylcyclohexan-1-one and 9.0 g (0.1 mole) of N-methoxycarbonyl hydrazine are dissolved in 100 cm3 of anhydrous ethanol, and the solution is boiled for 2 hours. Then it is cooled, and the separated crystals are filtered off. 18.2 g (96.9%) of the named compound are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04587261 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-22f0f84b0feb478f8e647024c2ae3d75 |
| 출처 메모 | uspto-grants-1986_05 |