Ammonia → D-Ribopyranosyl amine

HRID 279925

반응식

HRID 279925 반응식
O=[CH:2][C@@H:3]([C@@H:5]([C@@H:7]([CH2:9][OH:10])[OH:8])[OH:6])[OH:4].[Cl-].[NH4+:12].N>CO>[CH:9]1([NH2:12])[O:10][CH2:2][C@@H:3]([OH:4])[C@@H:5]([OH:6])[C@H:7]1[OH:8]

참가 물질

5

반응물 3

HCID 222AmmoniaHCID 25517Ammonium ChlorideHCID 5311110Aldehydo-D-ribose

생성물 1

HCID 54279899D-Ribopyranosyl amine수율 932.5%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To 100 ml of methanol was added 20 g of D-ribose and 0.5 g of ammonium chloride. This mixture was treated with anhydrous ammonia at 0° C. until a solution was obtained. This solution was stored at 0° C. for 13 days, then the solid was collected, giving 13 g of D-ribopyranosylamine.

후처리

  1. customwas obtained
  2. customthe solid was collected

출처 및 근거

ORD 기록
ord-6c82f99df2f64048a4c2ef165cd553e6
출처 데이터셋
uspto-grants-1986_05
특허 번호
US04587331

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