Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dibromosalicylic acid → N-[4-[1-(4-chlorophenyl)ethenyl]phenyl]-2-hydroxy-3,5-dibromobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dibromosalicylic acid | HCID 18464 | — |
| 반응물 | Phosphorus trichloride | HCID 24387 | — |
| 반응물 | 1-(4-Aminophenyl)-1-(4-chlorophenyl)ethylene | HCID 13608336 | — |
| 생성물 | N-[4-[1-(4-chlorophenyl)ethenyl]phenyl]-2-hydroxy-3,5-dibromobenzamide | HCID 13608338 | — |
반응 단계
Using the reaction conditions of Example 2, 5.92 g (0.02 mole) of 3,5-dibromosalicylic acid and 5.32 g (0.02 mole) of 1-(4-aminophenyl)-1-(4-chlorophenyl)ethylene in the presence of phosphorus trichloride were reacted to give 4.26 of purified N-[4-[1-(4-chlorophenyl)ethenyl]phenyl]-2-hydroxy-3,5-dibromobenzamide, m.p. 181°-183°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04587361 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-decb5f5514e0443994821db67f0a99e6 |
| 출처 메모 | uspto-grants-1986_05 |