Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
S-sec-butyl ethylphosphonotrithioic acid → 2-Butanethiol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | S-sec-butyl ethylphosphonotrithioic acid | HCID 13564051 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 2-Butanethiol | HCID 10560 | — |
| 생성물 | Phosphenodithioic ethane | HCID 16131073 | — |
반응 단계
Following the procedure as shown in Example 1, step (a), 14.67 g (94%) of the triethylamine salt of S-sec-butyl ethylphosphonotrithioic acid was obtained from 6.0 g (0.0242 mole) of ethylthionophosphine sulfide, 5.80 ml (4.58 g, 0.0508 mole) of sec-butyl mercaptan, and 7.1 ml (5.14 g, 0.0508 mole) of triethylamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04588714 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-8e63865f0003448689fe7282a09d16c0 |
| 출처 메모 | uspto-grants-1986_05 |