Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1'-Carbonyldiimidazole → 5-Pyrimidyl carboxylic acid imidazolide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 반응물 | Pyrimidine-5-carboxylic acid | HCID 78346 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 5-Pyrimidyl carboxylic acid imidazolide | HCID 86739966 | — |
반응 단계
5-pyrimidyl carboxylic acid, 1.9 gm, was added to 30 ml of methylene chloride. 2.4 gm of carbonyldiimidazole was added to the system. The system was stirred at room temperature for 3 hours to form the 5-pyrimidyl carboxylic acid imidazolide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04588735 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-45c587997494432c87f23050fd22982c |
| 출처 메모 | uspto-grants-1986_05 |