Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyrazine → 1-(2-Pyrazinyl)-2,2-dimethylpropanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyrazine | HCID 9261 | — |
| 반응물 | Pivalaldehyde | HCID 12417 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-(2-Pyrazinyl)-2,2-dimethylpropanone | HCID 546031 | 11% |
반응 단계
The reaction of pyrazine and trimethylacetaldehyde is conducted in the manner described in Example I on the same molar scale. Preparative thick layer chromatography (2000μ silica gel GF, developed with methylene chloride) of the crude reaction product provides an 11% yield of 1-pyrazinyl-2,2-dimethyl-1-propanone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04588813 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-78d20b627add4015a20ffd02abad92f2 |
| 출처 메모 | uspto-grants-1986_05 |