Thioglycolic Acid → Cyclooctyl mercaptoacetate

HRID 280498노트

반응식

HRID 280498 반응식
[CH:1]1([OH:9])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[SH:10][CH2:11][C:12](O)=[O:13].C1(C)C=CC(S(O)(=O)=O)=CC=1>>[SH:10][CH2:11][C:12]([O:9][CH:1]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)=[O:13]

참가 물질

4

반응물 3

HCID 1133Thioglycolic AcidHCID 6101p-Toluenesulfonic acidHCID 12766Cyclooctanol

생성물 1

HCID 20212358Cyclooctyl mercaptoacetate

실험 절차

Into a 100 ml reaction flask equipped with stirrer, thermometer, reflux condenser and heating mantle are placed 32 grams of cyclooctanol; 9.2 grams of mercaptoacetic acid and 0.5 grams paratoluene sulfonic acid.

후처리

  1. customInto a 100 ml reaction flask
  2. customequipped with stirrer
  3. temperaturethermometer, reflux condenser
  4. temperatureheating mantle

출처 및 근거

ORD 기록
ord-e02bfdc43ff3476392826e50b8b1bd94
출처 데이터셋
uspto-grants-1986_05
특허 번호
US04590082

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