Carbon Dioxide → 86792-71-4

HRID 280592노트

반응식

Br[C:2]1[CH:11]=[CH:10][C:5]2[S:6][C:7]([CH3:9])=[CH:8][C:4]=2[CH:3]=1.[C:12](=[O:14])=[O:13]>>[CH3:9][C:7]1[S:6][C:5]2[CH:10]=[CH:11][C:2]([C:12]([OH:14])=[O:13])=[CH:3][C:4]=2[CH:8]=1

참가 물질

반응물 2

HCID 280Carbon Dioxide

HCID 136630355-Bromo-2-methyl-1-benzothiophene

생성물 1

HCID 1366303686792-71-4

실험 절차

Conversion of 5-bromo-2-methylbenzo[b]thiophene to the Grignard reagent followed by reaction with carbon dioxide by the method of Example 3(i) gave 2-methylbenzo[b]thiophene-5-carboxylic acid, m.p. 220°-222°.

출처 및 근거

ORD 기록: ord-da5a92849d294440a8f44e56e1857232
출처 데이터셋: uspto-grants-1986_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04590200

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