Sodium Bicarbonate → 7-Bromo-2-dimethylaminomethyl-1-tetralone

HRID 280628노트

반응식

HRID 280628 반응식
Cl.[Br:2][C:3]1[CH:12]=[C:11]2[C:6]([CH2:7][CH2:8][CH:9]([CH2:14][N:15]([CH3:17])[CH3:16])[C:10]2=[O:13])=[CH:5][CH:4]=1.C(=O)(O)[O-].[Na+]>O>[Br:2][C:3]1[CH:12]=[C:11]2[C:6]([CH2:7][CH2:8][CH:9]([CH2:14][N:15]([CH3:17])[CH3:16])[C:10]2=[O:13])=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 516892Sodium BicarbonateHCID 233209337-Bromo-2-dimethylaminomethyl-1-tetralone hydrochloride

생성물 1

HCID 136630577-Bromo-2-dimethylaminomethyl-1-tetralone

시약·촉매·용매 1

HCID 962Water용매

실험 절차

The hydrochloride was converted to the free base by dissolving in a small volume of water and adding a slight excess of a saturated aqueous solution of sodium bicarbonate. Ether extraction gave the free base as an oil.

후처리

  1. extractionEther extraction

출처 및 근거

ORD 기록
ord-db0c8c3ecc994e628a5282a8005ae732
출처 데이터셋
uspto-grants-1986_05
특허 번호
US04590200

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