Trimethyl phosphite → HCID 23320145, 화합물

HRID 280860노트

반응식

HRID 280860 반응식
C[O:2][P:3]([O:6][CH3:7])[O:4][CH3:5].Cl[C:9]([O:11][CH:12]1[CH:19]2[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:21][CH:13]1[CH2:14]3)[CH2:18]2)=[O:10]>>[CH:19]12[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:21][CH:13]([CH2:14]3)[CH:12]1[O:11][C:9]([P:3](=[O:2])([O:6][CH3:7])[O:4][CH3:5])=[O:10])[CH2:18]2

참가 물질

3

반응물 2

HCID 8472Trimethyl phosphiteHCID 108785372-adamantyl Chloroformate

생성물 1

HCID 23320145HCID 23320145, 화합물

실험 절차

From 1.5 g (12 mmole) of trimethylphosphite and 2.0 g (9.3 mmole) of 2-adamantyl chloroformate: (100°-110° C., 2 hrs). Yield 1.0 g (37%). Bp0.3 160° C.

후처리

  1. custom(100°-110° C., 2 hrs)
  2. customBp0.3 160° C.

출처 및 근거

ORD 기록
ord-04ef689eb7bf4e53977789b4c44fb1ef
출처 데이터셋
uspto-grants-1986_05
특허 번호
US04591583

반응 노트

불러오는 중…