Hydroxylamine → p-Chlorobenzylmercaptoacetohydroxamic acid

HRID 28166

반응식

HRID 28166 반응식
[Cl:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][S:7][CH2:8][C:9](OC)=[O:10])=[CH:4][CH:3]=1.[NH2:15][OH:16].CO[Na]>CO>[Cl:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][S:7][CH2:8][C:9]([NH:15][OH:16])=[O:10])=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 787HydroxylamineHCID 3311340Methyl 2-(4-chlorobenzylthio)acetateHCID 178418582HCID 178418582, 화합물

생성물 1

HCID 54399917p-Chlorobenzylmercaptoacetohydroxamic acid

시약·촉매·용매 1

HCID 887Methanol용매2회

실험 절차

A solution of 0.15 mol of methyl p-chlorobenzylmercapto-acetate in 50 ml of methanol is mixed with a solution of 0.225 mol of hydroxylamine (base) and 0.15 mol of CH3ONa in 150 ml of methanol.

출처 및 근거

ORD 기록
ord-1fd68710babc4790bda705846fb1e0d5
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04225617

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