2-Acetylthiophene → 1-(4-Methyl-5-thiazolyl)-1-(2-thienyl)ethanol

반응식

[CH3:1][C:2]1[N:3]=[CH:4][S:5][CH:6]=1.[C:7]([C:10]1[S:11][CH:12]=[CH:13][CH:14]=1)(=[O:9])[CH3:8]>>[CH3:1][C:2]1[N:3]=[CH:4][S:5][C:6]=1[C:7]([C:10]1[S:11][CH:12]=[CH:13][CH:14]=1)([OH:9])[CH3:8]

참가 물질

반응물 2

HCID 69202-Acetylthiophene

HCID 127484-Methylthiazole

생성물 1

HCID 189363081-(4-Methyl-5-thiazolyl)-1-(2-thienyl)ethanol

실험 절차

Starting with 4-methylthiazole and 2-acetylthiophene and following the general method of Example 15 the title compound was prepared. M.p. 146.5°-147.5° C.

출처 및 근거

ORD 기록: ord-c5c6c64398c34e29931916d91cb3bfd4
출처 데이터셋: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05731335

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