Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Boron trifluoride | HCID 6356 | — |
| 반응물 | Azidotrimethylsilane | HCID 78378 | — |
| 반응물 | 1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol | HCID 9794153 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane | HCID 18936294 | — |
반응 단계
1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol (1 g) was suspended in benzene (4 ml). Trimethylsilylazide (822 μl) was added followed by boron trifluoride diethyletherate (770 μl). The mixture was stirred overnight at room temperature, then poured into water and extracted to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731335 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-d5df902db51f4973b3595b8e30064e32 |
| 출처 메모 | uspto-grants-1998_03 |