Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylamine → Acetoacetamide, N,N-diethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | Ethyl Acetoacetate | HCID 8868 | — |
| 생성물 | Acetoacetamide, N,N-diethyl- | HCID 16699 | 65.7% |
반응 단계
40 g (0.31 mol) of ethyl acetoacetate and 24 g (0.33 mol) of diethylamine were stirred in a Parr apparatus at 150° C. for 10'. The crude mixture was distilled at 115°-120° C./9 mmHg, to give 32 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-51c44092234a4bbebe6940b7ac132c46 |
| 출처 메모 | uspto-grants-1998_03 |