Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178418442, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Benzenediazonium chloride | HCID 60992 | — |
| 반응물 | 3-Oxo-n,n-dipropylbutanamide | HCID 249207 | — |
| 반응물 | HCID 178418247 | HCID 178418247 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178418442 | HCID 178418442 | 14.5% |
반응 단계
18.5 g (0.1 mol) of N,N-dipropyl-3-oxobutyramide, 12 g (0.146 mol) of CH3COONa, 20 ml of water, 75 ml of ethanol and a solution of 0.1 mol of phenyldiazonium chloride were treated as described in preparation 2. The precipitated solid was filtered and dried in vacuo yielding 4.2 g of the title compound. M.p.=79°-80° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-549c90cb2eaf4302a24586469500c664 |
| 출처 메모 | uspto-grants-1998_03 |