Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178418235, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Benzenediazonium chloride | HCID 60992 | — |
| 반응물 | Isobutyl acetoacetate | HCID 522677 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178418235 | HCID 178418235 | 88.1% |
반응 단계
15.8 g (0.1 mol) of i-butyl acetoacetate, 12 g (0.146 mol) of CH3 COONa, 20 ml of water, 75 ml of ethanol and a solution of 0.1 mol of phenyldiazonium chloride were treated as described in preparation 2. The precipitated solid was filtered an dried in vacuo yielding 23.1 g of the title compound. M.p.=45°-50° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-eb91f88045c44fa2ba05b793165e13a8 |
| 출처 메모 | uspto-grants-1998_03 |