Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → N-benzyl-3-oxo-2-(phenylhydrazinylidene)butanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Benzenediazonium chloride | HCID 60992 | — |
| 반응물 | Acetoacetobenzylamide | HCID 70159 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-benzyl-3-oxo-2-(phenylhydrazinylidene)butanamide | HCID 178418323 | — |
반응 단계
7.27 g (0.038) of N-benzyl-3-oxobutyramide were dissolved in a solution of 5.32 g (0.133 mol) of NaOH in 58 ml of water. To the ice-cooled stirred solution, 0.040 mol of phenyldiazonium chloride were added dropwise at such a rate as to keep the temperature at 0° C. The precipitated solid was filtered and recrystallised from MeOH yielding 9 g of the title compound. M.p.=101°-103° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-24aef19954464872a4172777d7b361e8 |
| 출처 메모 | uspto-grants-1998_03 |