Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetoacetanilide → HCID 178418293, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetoacetanilide | HCID 7592 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Benzenediazonium chloride | HCID 60992 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178418293 | HCID 178418293 | 47.6% |
반응 단계
4.5 g (25.4 mmol) of acetoacetanilide, a solution of 3.46 g (89 mmol) of NaOH in 45 ml of water and 95 mmol of phenyldiazonium chloride were treated as described in preparation 8. The residue was crystallised from EtOH, yielding 3.4 g of the title compound. M.p.=96°-97° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-f388a24479e44c98bc290884466e1ad3 |
| 출처 메모 | uspto-grants-1998_03 |