Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → Dimethylacetoacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Diketene acetone | HCID 87118046 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Dimethylacetoacetamide | HCID 16278 | — |
반응 단계
A solution of 9 ml (0.05 mmol) of diketene-acetone adduct in 20 ml of toluene was treated with gaseous dimethylamine at room temperature until the reaction was complete. The solvent was removed in vacuo and the residue was purified by chromatography on silica gel (EtOAc/MeOH 0%→10%) yielding 7.0 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-eb592b1203c74e969732293b7513ee02 |
| 출처 메모 | uspto-grants-1998_03 |