Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → HCID 178418269, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Benzenediazonium chloride | HCID 60992 | — |
| 반응물 | 3-Oxo-N,N-di(propan-2-yl)butanamide | HCID 12318541 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178418269 | HCID 178418269 | 68.2% |
반응 단계
7.0 g (0.038 mol) of N,N-diisopropyl-3-oxobutyramide, a solution of 5.3 g (0.133 mol) of NaOH in 58 ml of water and 0.04 mol of phenyldiazonium chloride were treated as described in preparation 8. The crude reaction mixture was purified by chromatography on silica gel (hexane/Et2O 95:5) obtaining 7.5 g of the title compound which was used as such in the subsequent step. M.p.=143°-145° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731322 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-ee71b009ed3f4c28bab5abd1c42abd9d |
| 출처 메모 | uspto-grants-1998_03 |