Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine → N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-N'-[4-(dimethylamino)phenyl]urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine | HCID 597879 | — |
| 반응물 | 4-(Dimethylamino)phenyl isocyanate | HCID 2733372 | — |
| 생성물 | N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-N'-[4-(dimethylamino)phenyl]urea | HCID 11304884 | — |
반응 단계
N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-N′-[4-(dimethylamino)phenyl]urea was prepared from 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine and 4-dimethylamino phenyl isocyanate in a similar manner as described above to give a tan solid (40% yield). 1H-NMR (DMSO-d6): δ 10.99 (s, 1H), 7.98 (s, 1H), 7.60 (d, 1H), 7.33-7.23 (m, 3H), 7.17 (dd, 1H), 6.71 (d, 2H), 6.44 (d, 1H), 5.00 (m, 1H), 2.84 (s, 6H), 2.67 (m, 2H), 2.04 (m, 1H), 1.94-1.74 (m, 3H); MS m/z 427 (M−1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07419997B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-fb607263e894452a9a4c3aef4d7b0b66 |
| 출처 메모 | uspto-grants-2008_09 |